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Applying scanning probe microscopy to study morphology of solid surfaces
Technical sciences

Authors: Daria Yu. KHANUKAEVA graduated from Moscow Institute of Physics and Technology in 1999, she is Candidate of Physico-Mathematical Sciences, Associate Professor of the Department of Higher Mathematics. She is author of more than 30 publications in the field of mechanics and mathematics. E-mail khanuk@yandex.ru
Anatoly N. FILIPPOV (b. 1960) graduated from Lomonosov Moscow State University in 1982. He is Doctor of Physico-Mathematical Sciences, рrofessor of the Department of Higher Mathematics. He is author of more than 300 publications and 3 monographs in the fields of physicochemical mechanics, colloid chemistry and mathematics. E-mail filippov.a@gubkin.ru
Vladimir I. IVANOV (b. 1961) graduated from Lomonosov Moscow State University in 1983. Нe is Candidate of Physico-Mathematical Sciences, аssociate Professor of the Department of Higher Mathematics. He is author of more than 10 publications in the fields of physicochemical, hydrodynamics, colloid chemistry and mathematics. E-mail vladimir.i-ivanov@yandex.ru
Vasily V. KALININ (b. 1952) graduated from Lomonosov Moscow State University in 1974. He is Doctor of Physico-Mathematical Sciences. Head of the Department of Higher Mathematics. He is author of more than 70 publications in the fields of physicochemical hydrodynamics, colloid chemistry and mathematics. E-mail vm@gubkin.ru

Abstract: Five different examples of the use of scanning probe microscopy to study the morphology of solid rough surfaces were studied. These demonstrated the potential of a variety of AFM techniques. All these measurements were carried out on areas of micron-scale of the parts and pieces of research objects, which are geological materials, metal samples and polymer membranes with sizes down to a few nanometers. These results are related to the micro- and nanostructures of the materials studied and allow gathering information about their properties in these scales, thus opening up opportunities for the development of new models and technologies.

Index UDK: УДК 532.546.2

Keywords: atomic force microscopy, surface morphology, roughness, porous structure, minerals, polymeric membranes.

1. Khanukaeva D.Yu., Filippov A.N., Bildyukevich A.V. An AFM Study of Ultrafiltration Membranes: Peculiarities of Pore Size Distribution. Petroleum Chemistry, 2014, vol. 54, no. 7, p. 498–506.
2. Jesse S., Kalinin S.V. Band excitation in scanning probe microscopy: signs of change. J. Phys. D: Appl. Phys., 2011, vol. 44, p. 464006–464022.
3. Khanukaeva D.Yu., Kalinin S.V., Filippov A.N., Ievlev A.V., Buzilov A.S. Scanning probe microscopy of minerals microstructure. Metodologicheskie aspecty scaniruyushchei zondovoi microscopii — BelSZM XI [Proc. XI Int. Conf. „Methodological Aspects of Scanning Probe Microscopy”]. Minsk, 2014, p. 178-183 (in Russian).
4. Chen C.-Y., Garnica-Rodrigues J.I., Duke M.C., Dalla Costa R.F., Dicks A.L., Diniz da Costa J.D. Nafion/polyanilin/silica composite membranes for direct methanol fuel cell application. J. of Power Sources, 2007, vol. 166, p. 324-330.
5. Kolechko M.V., Filippov A.N., Shkirskaya S.A., Timofeev S.V., Berezina N.P. Synthesis and Diffusion Permeability of MF-4SK/Polyaniline Composite Membranes with Controlled Thickness of the Modified Layer. Colloid Journal, 2013, vol. 75, no. 3, p. 289-296.
6. Kalinin V.V., Filippov A.N., Khanukaeva D.Yu. Investigation of Membrane Morphology by Atomic Force Microscopy Under Mathematical Modeling of Diffusive Processes. Trudy RGU nefti i gaza imeni I.M. Gubkina [Proceedings of Gubkin Russian State University of Oil and Gas], 2012, no. 1 (266), p. 129-136 (in Russian).
7. Filippov A., Afonin D., Kononenko N., Shkirskaya S. Characterization of Perfluorinated Cation-Exchange Membranes MF-4SC Surface Modified with Halloysite Nanotubes. AIP Conf. Proc. AMiTaNS’15″, 2015, vol. 1684, p. 030004-1-030004-9.
8. Filippov Anatoly, Khanukaeva Daria, Afonin Denis, Skorikova Galina, Ivanov Evgeny, Vinokurov Vladimir and Lvov Yuri. Diffusive Permeability of Hybrid Cation-Exchange Membranes MF-4SC/Halloysite Nanotubes. Proc. of IEEE, 15th International Conference on Nanotechnology (IEEE-NANO) (Rome, Italy, 27-30 July 2015), 2015 IEEE, p. 208-211.
9. Khanukaeva D.Yu., Filippov A.N. Statistical Processing of Ultrafiltration Membrane Pore Size Distribution Determined by Atomic Force Microscopy. Petroleum Chemistry, 2015, vol. 55, no. 10, p. 909-917.
10. Gwyddion, http://gwyddion.net/