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2015/4
Possibilities of mid-ir-spectroscopy to analyze diesel fuels
Chemical sciences

Authors: Olga V. PRIMEROVA graduated from Gubkin Russian State University of Oil and Gas in 2015. Еngineer of department of Organic chemistry and petroleum chemistry of the Gubkin Russian State University of Oil and Gas, author of 18 publications in the field chemistry of oil. E-mail: Primerova92@yandex.ru
Ludmila V. IVANOVA graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1983. She is Associate Professor of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. She has authored 98 scientific publications in the field of chemistry of oil. E-mail: ivanova.l@gubkin.ru
Vladimir N. KOSHELEV born in 1953. He graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1975. He is Vice Rector for Academic Affairs, Head of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. He is author of over 310 scientific papers in the field of organic and petroleum chemistry.
E-mail: koshelev.v@gubkin.ru
Yegor A. BUROV was born in 1987. Нe defended his Master’s thesis at Gubkin Russian State University of Oil and Gas in 2010. He is presently a postgraduate student of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. He has authored 21 scientific publications in the field of chemistry of oil. E-mail: burov_egor48@mail.ru
Alexey V. YUSOVSKY born in 1994. Student of oil Processing Technologies department of the Gubkin Russian State University of Oil. Author of 2 publications in the field chemistry of oil. E-mail: Jusovskijj94@yandex.ru

Abstract: The possibilities of infrared spectroscopy in the analysis of the hydrocarbon composition of diesel fuel are described and relationships between the composition and properties are established. The focus is on detailed study of the structure of paraffin and naphthenic hydrocarbons and their influence on the low temperature properties of diesel fuels e.g. filterability limit temperature and pour point. The data on various functional additives presence in diesel fuel are represented. Calibration curves to determine the concentration of additives are constructed. It is shown that the intensity of the characteristic band of the functional groups in the additive package is lower than that in solutions of individual additives

Index UDK: УДК 665.75:543.068.8

Keywords: IR spectroscopy, diesel fuel, hydrocarbon composition, low temperature properties, content of additives in fuels

Bibliography:
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2.Vasilenko P.A. Apparaturno-metodicheskij kompleks dlja izmerenij soderzhanija primesej v mnogokomponentnyh uglevodorodnyh rastvorah IKAR-3. Geopolitika. Georesursy. Geojenergetika, 2010.
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5.Glebovskaja
E.A., Maksimov Je.I., Petrov A.K. Kolichestvennoe opredelenie SN2-grupp v otkrytyh cepjah s chislom zven’ev ne menee chetyreh. Zhurnal analiticheskoj himii, 1959, tom 24, vyp. 4, p. 478-481.
6.Alessandra Borin, Ronei J. Poppi. Application of mid infrared spectroscopy and iPLS for the quantification of contaminants in lubricating oil. Vibrational Spectroscopy 37 (2005) 27–32.
7.Boris
Mizaikoff. Fuel Performance Specifications, Mid-infrared Analysis. Encyclopedia of Analytical Chemistry. R.A. Meyers (Ed.), 2000.
8.Berthold P., Staude V., Bernhard U. IR-spektrometrische Strukturgruppeanalyse aromatenbaltiger Mineralolprodukte. Schmierungstechnik, 1976, no. 7, p. 280.

2013/1
Petroleum Acids and their Derivatives. Manufacturing and Application (an overview)
Oil and gas processing, chemistry of oil and gas

Authors: Ludmila V. IVANOVA graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1983. She is Associate Professor of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. She has authored 52 scientific publications in the field of chemistry of oil. E-mail: ivanova.l@gubkin.ru
Vladimir N. KOSHELEV born in 1953. He graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1975. He is First Vice Rector for Academic Affairs, Head of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. He is author of over 280 scientific papers in the field of organic and petroleum chemistry. E-mail: koshelev.v@gubkin.ru
Nina A. SOKOVA graduated from Gubkin Moscow Oil Institute in 1957. She is Associate Professor of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. She has authored 20 scientific publications in the field of chemistry of oil. E-mail: sokova.n@gubkin.ru
Yegor A. BUROV was born in 1987, he defended his Master’s thesis at Gubkin Russian State University of Oil and Gas in 2010. He is presently a postgraduate student of the Department of Organic Chemistry and Petroleum Chemistry of Gubkin Russian State University of Oil and Gas. He has authored 8 scientific publications in the field of chemistry of oil. E-mail: burov_egor48@mail.ru
Olga V. PRIMEROVA is a student of the Faculty of Chemical and Environmental Engineering at Gubkin Russian State University of Oil and Gas. E-mail: feekys@gmail.com

Abstract: An overview of the main sources, methods of separation and applications of petroleum acids is presented. While petroleum acids are widely applied in various fields of economy, their natural resources are currently limited. Finding oils rich in petroleum acids in the Russian oilfields is a pressing problem. The list of sources includes 37 references to the publications and dissertations in the field of interest.

Index UDK: 665.6

Keywords: petroleum acids, naphthenic acids, derivatives of naphthenic acids, manufacturing of naphthenic acids, properties of naphthenic acids, application of naphthenic acids

Bibliography:
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2011/4
Peculiarities of Asphaltene-Resin-Paraffin Deposits in Late Stages of Field Development
Oil and gas processing, chemistry of oil and gas

Authors: Lyudmila V. IVANOVA graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1983. She is Associate Professor of the Department of Organic Chemistry and Petroleum Chemistry at Gubkin Russian State University of Oil and Gas, author 52 scientific works in the field of petroleum chemistry. E-mail: ivanova.l@gubkin.ru
Vladimir N. KOSHELEV was born in 1957, graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1975. He is First Vice-Rector for Academic Affairs, head of the Department of Organic Chemistry and Petroleum Chemistry at Gubkin Russian State University of Oil and Gas, author of more than 280 scientific papers in the field of organic chemistry and petroleum chemistry. E-mail: koshelev.v@gubkin.ru
Alexey A. VASECHKIN was born in 1986, graduated from Gubkin Russian State University of Oil and Gas in 2008. He is postgraduate student of the Department of Organic Chemistry and Petroleum Chemistry at Gubkin Russian State University of Oil and Gas. He is author of 8 scientific papers and publications in the field of oil study. E-mail: vasexhkin.aleksey@yandex.ru
Yegor A. BUROV was born in 1987, graduated from the Master Program of Gubkin Russian State University of Oil and Gas in 2010. He is now postgraduate student of the Department of Organic Chemistry and Petroleum Chemistry at Gubkin Russian State University of Oil and Gas, author of 8 scientific papers in the field of oil study. E-mail: burov_egor48@mail.ru
Olga V. PRIMEROVA is a student the Faculty of Chemical Engineering at Gubkin Russian State University of Oil and Gas. E-mail: feekys@gmail.com

Abstract: The paper analyzes the influence of the chemical composition of a group of four oils of Volgograd and Orenburg regions on their low temperature properties: freezing point and the tendency to form asphaltene-resin-paraffin deposits. It is shown that when studying the group composition it is important to consider not only the quantitative content of individual groups of compounds: paraffin-naphthenic and aromatic hydrocarbons, resins and asphaltenes in the oil, but also their mutual relationship, which can be determined on the basis of spectral coefficients. We found that deposits may grow in the presence of formation water. This is due to the amount of polar components-resins and asphaltenes - in the studied oil.

Index UDK: 622.276

Keywords: asphaltene-resin-paraffin deposits (ARPD), structural-group composition, physical and chemical properties of oil, IR spectra, spectral coefficients of oil, water cut

Bibliography:

2010/2
Applying ir-spectrometry to study oils
Oil and gas processing, chemistry of oil and gas

Authors: Lyudmila V. IVANOVA was born in 1961, graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1975. She is assistant professor of the Department of Organic Chemistry and Chemistry of Oil at Gubkin Russian State University of Oil and Gas, author of 37 publications. E-mail: ivanova.l@gubkin.ru
Vladimir N. KOSHELEV was born in 1953, graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1983. He is Vice Rector for Petroleum Engineering Education, head of the Department of Organic Chemistry and Chemistry of Oil at Gubkin Russian State University of Oil and Gas. He is the author of over 253 publications in the field of organic chemistry and chemistry of oil. E-mail koshelev.v@gubkin.ru
Egor A. BUROV was born in 1987. He is studying for master’s degree in “Chemical Engineering for Oil Production” at Gubkin Russian State University of Oil and Gas, published 2 works in the field of oil studies. E-mail: burovegor48@mail.ru
Olga A. STOKOLOS was born in 1971, graduated from Gubkin Moscow Institute of Petrochemical and Gas Industry in 1975. She is assistant professor of the Department of Organic Chemistry and Chemistry of Oil at Gubkin Russian State University of Oil and Gas, author of 8 publications in the field of chemistry of oil. E-mail: stokolos.o@gubkin.ru

Abstract: IR-spectrometry is a most informative and sensitive method of studying the composition and structure of organic compounds. Oil systems being multi-component, IR-spectrometric study reduces to determining different groups of compounds in the composition of oil and their interrelationship. Oils obtained from different fields of Russia and Kazakhstan were studied using IR-Fourier - spectrometry. Hydrocarbon type content and spectral factors were calculated

Index UDK: 543.42:543.544.45: 665.61

Keywords: IR-spectrometry, hydrocarbon type content, hydrocarbon spectral factors

Bibliography: